NSC 60136
3-Chloropropionaldehyde diethyl acetal
CAS: 35573-93-4
Molecular Formula: C7H15ClO2
NSC 60136 - Names and Identifiers
| Name | 3-Chloropropionaldehyde diethyl acetal |
| Synonyms | NSC 60136 3-chloro-1,1-diethoxypropane 3-CHLORO-1,1-DIETHOXYPROPANE 3-chloro-1,1-diethoxy-propan β-Chloropropanal Diethyl Acetal Propane, 3-chloro-1,1-diethoxy- 3-Chloropropionaldehyde diethyl acetal B-CHLOROPROPIONALDEHYDE DIETHYL ACETAL Propionaldehyde, 3-chloro-, diethyl acetal 3-Chloroprionaldehyde Diethyl Acetal, Technical grade 1-Chloro-3,3-diethoxypropane~3-Chloropropanal diethyl acetal |
| CAS | 35573-93-4 |
| EINECS | 252-623-4 |
| InChI | InChI=1/C6H14O2.C3H5ClO/c1-4-7-6(3)8-5-2;4-2-1-3-5/h6H,4-5H2,1-3H3;3H,1-2H2 |
| InChIKey | NXHONHDWVLPPCS-UHFFFAOYSA-N |
NSC 60136 - Physico-chemical Properties
| Molecular Formula | C7H15ClO2 |
| Molar Mass | 166.65 |
| Density | 0.995g/mLat 25°C(lit.) |
| Boling Point | 84°C25mm Hg(lit.) |
| Flash Point | 98°F |
| BRN | 1698609 |
| Storage Condition | 2-8°C |
| Refractive Index | n20/D 1.42(lit.) |
| Physical and Chemical Properties | Irritating flammable liquid. The boiling point is 84 degrees C (3.33kPa), the relative density is 0.995, and the refractive index is 1.4200. Insoluble in water, soluble in alcohol, ether. |
NSC 60136 - Risk and Safety
| Risk Codes | R10 - Flammable R36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. S16 - Keep away from sources of ignition. |
| UN IDs | UN 1989 3/PG 3 |
| WGK Germany | 3 |
| FLUKA BRAND F CODES | 10-21 |
| HS Code | 29091990 |
| Hazard Class | 3 |
| Packing Group | III |
NSC 60136 - Reference Information
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| use | for organic synthesis. |
| production method | add precooled acrolein dropwise to precooled anhydrous ethanol-hydrogen chloride saturated solution for reaction. The reactants are divided into two layers, separated from the lower acetal, neutralized with powdered sodium bicarbonate, and filtered. The filtrate is washed with ice water, dried, distilled under reduced pressure, and the fraction at 58-62 ℃(1.07kPa) is collected to obtain the product. The yield is 34%. |
Last Update：2024-04-09 15:16:45
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